the Wake Forest University - Nano and Quantum Technologies Laboratory
NanoteQ
Molecular Beam Epitaxy Core
MBE
The NanoteQ system is based on the Scienta Omicron LAB10 MBE system with Auger, LEED, and STM as added surface analysis tools. This system (an example is shown above) is setup for Ga, As, In, Sb, Bi, Te, and Al. But, it can be reconfigured for a variety of other systems.
The MBE Core lab centers on the creation of Nano-Materials, Quantum Materials, Low Dimensional Materials and other Exotic solids using the techniques of MBE.
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Molecular beam epitaxy (MBE) means creating a single crystal by building up orderly layers of molecules on top of a substrate or base layer.
To make an interesting new 2D crystal using MBE, you start with a a substrate of some familiar material such as silicon, germanium, or gallium arsenide, with an atomically flat surface. Then to prepare for the addition of more layers, you heat the substrate to hundreds of degrees (for example, 500–850°C or about 930–1560°F in the case of gallium arsenide).
To add the "new crystalline" layer, you fire relatively precise beams of atoms or molecules (heated up so they're in gas form) at the substrate from small evaporative sources called effusion cells. The effusion cell is open at one end and consists of a tapered crucible filled with the material it's going to evaporated, an electrically controlled heater, and a thermocouple for measuring and regulating the temperature.
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The number and type of cells depends on the complexity of the crystal being produced; there can be as many as 8–14 of them. Like the substrate, the cells are heated to high temperatures—a maximum of about 1500–1600°C or so (2700–2900°F).​​​​​​​​​​​​​​​​​​
Materials Processing
​NanoteQ also offers a broad range of growth and materials processing capabilities. As with any such Nano-Lab, experiments start with excellent control over the materials.
High temperature centering and forming ovens
Chemical Synthesis
The synthesis lab has capabilities that allow for the creation of conjugated polymers used in OLED and OPV device studies to 2D inorganic chalcogenide topological materials.
Multiple solvent stills
Glovebox for air/moisture sensitive reactions
Ultra-fine glovebox Scales
A large assortment of glassware and reactors
Cold chemical storage
Rotovap
Closed circuit chiller system
microwave reactors
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